GCMS analysis comments for sample AD29134, Dec 17 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29134.D Vial: 10 Acq On : 10 Dec 2001 7:31 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.71 ug/1 . 187598 1,4-Dichlorobenzene-d4 11.67

Hit# Of Tentative ID 5 MW MolForm CAS# Qual 1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 56 3 2-Propanol, 1-(/-methoxypropoxy) - 148 C7H1603 013429-07-7 38 4 1-Propanol, 2-/2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 33 {Abundance Scan 695 (11.429 mln): 29134.D (-) m/z 59.05 100.00% 59

mz-? 5000

20 —10—1 45

391. — I ■ 14 ■ ■ ■ ' TN* ‘ I ‘ ' ‘I ‘ 30 40 50 60 70 73

80 90 100 110 120 103

11 — . ।।। ।। . 130 140 111 11.00 11.20 11.40 11.60 11.80 m/z N 45.05 • • i ■ ■

47.82% Abundance ' 3#9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59 5000 103 • i < । • i । > • « i » • 45 73 11.00 11.20 11.40 11.60 11.80 31 m/z 103.05 39.56% ■ ■I........... . ............................. •i■■■1 I ‘ ‘ 1 ■ l' 111 — miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance ' #12359: 2-Butanol. 3,3’-oxybis- 59 11.00 11.20 11.40 11.60 11.80 5000

m/z-> Abundance 31

■ । ■ ■ ■ ■ । 20 30 ' * • i1 40 45

50 1eo— 70 180 90 100 110 120— 130 140 #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59 103

13 11.00 11.20 11.40 11.60 11.80 m/z

m/z A 73.00

41.05 28.17%

24.58% 5000

m/z—> 31 45 ----------- 20 30 40 50 60 70 73 _130 • i 1 ' ‘ ‘ i ‘ ' 1 ‘ I ■ • ' • i ■ 1 ■ ■ i ' ■ ■ ‘ i 1 ' • • i ■ ■ ■ ■ i ‘ 80 90 100 404

110 120 130 NUA 11T 1 ! 1021//1-r*111/nI 140 11.00 11.20 11.40 11.60 11.80

29134.D GCMS1126.M Wed Dec 12 16:05:54 2001 Page 3

NYC-WTC_000035874