GCMS analysis results sample AD29458, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\1\DATA\DEC1201\29458.D Vial: 30 Acq On 13 Dec 2001 6:16 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.64 ug/1 190549 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1 ,Y‘ -oxybis- 134 C6H14O3 000110-98-5 50 3 2-Butanol, 3 ,3 ‘ - oxybi s- 162 C8H18O3 054305-61-2 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance Scan 686 (11,339 min): 29458.D (-) m/z 59.05 100.00% I 59

5000

— 45 73 103 N 11.00 11.20 11.40 11.60 —60mt m/ z 44.95 51.69% m/z-> 20 30 40 50 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 34.96% • i ■ > • • i ■ ■ • ■ । • i ..... , ............................. ।..........—130 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol. 1,1‘-oxybis- 59 I - J- - I ‘ • 1 • I 11.00 11.20 11.40 11.60 31 5000- 45 m/ z 73.00 L ____ 27.56%

m/z-> Abundance 20 30 40 50 T1 60 72 • i ■ ■ 70 80 90 89

100 103

#12859: 2-Butanol, 3,3’-oxybis- 59 110 120 130 140

m/z NA 11.00 11.20 11.40 11.60 ^1-05 C5.73. 25.78%

m/z-> 5000

-------- 20 30 40 50 31 45

—mm 60 70 80 90 103

100 ..... 134 110 120 130 140 NA —11,1,,, ............. 1 11.00 11.20 11.40 11.60

29458.D GCMS1126.M Fri Dec 21 12:25:22 2001 Page 2

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