GCMS analysis comments, sample AD29025, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29025.D Vial: 29 Acq On 11 Dec 2001 3:59 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.59 ug/1 160601 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3‘- oxybi s- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1, 1 ‘ -oxybis- 134 C6H14O3 000110-98-5 50 4 2-Propanol/ - 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 Abundance Scan 686 (11.343 min): 29025.D (-) m/z 59.05 100. 00% 59 45 5000: 103 73 11.00 11.20 11.40 11.60

m/z-> 20 • i .... i . 30 39 ii

40 + 1IIm 50 4 60 .....70+— 80 84....... ।................. 90 100 110 120 130 140 m/z 44.95 49.84% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000- • t • • । ■ । ■ ■ ■ ■ । 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 34.01% ----- ■ i 1 * T । I ■ ■ ■ ■i 1 ■ ■ ' I ■ ' ■ * i ■ ,.......................130........... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3°oxybis- 59 1— 11.00 11.20 11.40 11.60 5000 31 m/z 73.00. 27.66% 45 103 i i il 134 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1‘-oxybis- ■ i ■ ' ' ' i 59 11.00 11.20 1140 ■ 11.60 m/ Z 41.00 25.26%

m/z-> 5000-

- — 20 31

30 40 45

■ I •

I50 17 •

I60 70 80 90 • । • i ■ ■ । 100 103

110 < I i।। T 120 130 140 —Pr NA ' ' I ' • ' ' I ' ' ' ' I 11.00 11.20 11.40 11.60

29025.D GCMS1126.M Wed Dec 12 15:45:31 2001 Page 3

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