GCMS analysis comments, sample AD29025, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29025.D Vial: 29 Acq On 11 Dec 2001 3:59 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.51 ug/1 136959 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, >1, 1,1-trichloro- 160 C3H3C130 000918-00-3 33 2 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 16 3 1 -Pentadecene 210 C15H30 013360-61-7 9 4 1-Hexadecanol 242 C16H340 036653-82-4 9 Abundance Scan 294 (7.744 min): 29025.D (-) m/z 43.05 100.00% 43

5000-

- । । । । > । TIT i । । । । । । 63 82 97 125 7.40 7.60 7.80 8.00 ii, , I L li ,, 11 207 ■ ' I ' ■ ' ■ i 1 ' ■ T i ' ' ' ■ i । ■ ■ 1 i ■ ■ ■ 'I ' 1 ' ' i ' ' ■ ' i 1 m/z 124.95 9.72% m/z—> 20___ 40 60 80 100 120 140___ 160 180 200 Abundance #12247: 2-Propanone, 1.1,1-trichloro- 43

5000 7.40 7.60 7.80 8.00 15 . m/z 96.95 7.91% I ....... 85 97 .....125 .................... ■ ' i ' m/z—> 20 40 60 80 100 120 140 160 180 200 Abundance #64841: 2-Propanone. 1,1-dichloro- 43 1...... 7.40 7.60 7.80 8.00 5000 m/z 126.90 7.83%

27... 63 83 ... . ............. m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #70191: 1-Pentadecene T i 1 1 1 1 11 1 TELL 1 I 1 ' ' ' I 43 69 83 97 7.40 7.60 7.80 8.00 57 m/z 46.95 7.19% 5000 111

125 — ........... 182.....210 i • ■ ■ ■ i ' 1 i ' ' 1 ' I ' ' ' ' I 1 1 1 1 I ' 1 1 1 I m/z-> 20 40 60 80 100 120 140 160 180 200 7.40 7.60 7.80 8.00

29025.D GCMS1126.M Wed Dec 12 15:45:27 2001 Page 2

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