GCMS analysis comments, sample AD29028, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29028 .D Vial: 32 Acq On : 11 Dec 2001 6:55 pm Operator: 209 GALOS Sample : gc/ms scan 11/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.61 ug/1 165529 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1.1, 1-trichloro- 160 C3H3C130 000918-00-3 37 2 Acetic acid, sec-octyl ester 172 C10H20O2 054515-77-4 25 3 1-Hexadecanol 242 C16H34O 036653-82-4 9 4 1-Octadecanol 270 C18H380 000112-92-5 9 Abundance Scan 294 (7.744 min): 29028.D (-) m/z 4 .95 100.00% 43

5000 1 ‘ • i • • ■ ■ i • • • • i • • • ■ i 53 83 97 125 7.40 7.60 7.80 8.00 । ■ i ■11 "I 1 w , , i. , L - m/z 124.95 8.31% miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 7.40 7.60 X T 7.80 8.00 m/z 82.8,5 7.49% 15 85 97 125 mz-> 20 40160 80 100 120 140 160 180 200 220 Abundance #15771: Acetic acid, sec-octyl ester 43 a... A 7.40 7.60 7.80 • i 1 • • • t 8.00 5000 87 m/z 126.90 6.80%

58 70 112 102 128 172 । - i | > rr i । । . i i i । i i । । . miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #71247:1-Hexadecanol — ——— • ■ i ■ ■ ' ■ i 43 — 7.40 7.60 7.80 8.00 55 m/z 96.95 5.65% 5000 83 27 70 97

mz—> 1 1 I 11 1 1 1 20 40 1 ( • 60 ■ 1 i' 80 -1125 100 120 . . । I . . 1 | I T-T I | . . . 1 | . . . . | I . 140 160 180 196 200 224 220 1 • i • ■ ■ ■ i 1 • ‘ * i ■ • • ' i ■ ■ 7.40 7.60 7.80 8.00 • i

29028.D GCMS1126.M Wed Dec 12 15:49:37 2001 Page 2

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