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Document / 22 pages

GC/MS calibration data for sample 30645, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018470–000018491

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018476
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 7.75 0.62 ug/1 254898 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 4-Penten-2one 84 C5H80 013891-87-7 9 3 Ethanol,2, 2,2-trichloro- 148 C2H3C130 000115-20-8 9 4 Propionic acid, 2f2-dichloro-, pent 212 C8H14C12O2 017640-08-3 9 Abundance ‘ Scan 295 (7.753 mln): 30645.D (-) m/z 4 .05 100.00% 43

5000 । r .r . 35 49 63 69 75 83. 97, 117 125 7.40 7.60 7.80 8.00 • • ।1 ■ ■ ■ । • ■ ■ ■ । ■ - t 11′1 >.., ;»1'| 11-| ■ f.. [ |K‘1 ■ 111 r r" . 1 I'. ■ .'.'I i teep ■ 1 m/z 124.95 9.22% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 ’ * I ‘ ‘ ‘ * I * ’ 1 * I * ‘ ‘ ‘ I • 1 i • 7.40 7.60 7.80 8.00 15 m/z 46.95 7.06% 1 35 49 85 97 117 125 miz-> 10 20 30 40 50 60 ' ‘ 70 80 90 100 110 120 ′ 130 Abundance 43 #555: 4-Penten-2-one wWN WWAous • ■ i ■ ■ 1 1 i 1 111 114 i r ‘ । । ‘ i 7.40 7.60 7.80 8.00 5000 m/z 82.90 6.67% 15 ‘1****1** • ■ i • ■ ■ • 37 l; ‘ 53 69 ' i ■ ■ • • i • • •' i ‘ ——84mmmmmpT miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 31 #9118: Ethanol, 2,2,2-trichloro- MAAAAALMMAAA 7.40 7.60 7.80 8.00 m/z 126.90 6.52% 5000 49 77 A.................... \/\.................... | 84 113119 97 m/z-> ••।• 10 1 20 30 40 I50 . 60 70 pla r j । « t । j > i > । । । i । i i i i । i r 80 90 100 110 120 130 111 •1 ‘ • i ■ •f• i1111111 r1 7.40 7.60 7.80 8.00

30645.D GCMS1126.M Fri Feb 01 10:52:32 2002 Page 2

NYC-WTC_000018476

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NYC-WTC_000018476Source: NYC Law Department, mirrored locally

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