GCMS analysis results for sample AD31405, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JANI602\31405.D Vial: 11 Acq On : 16 Jan 2002 9:25 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.59 0.92 ug/1 236211 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 - Propanone', 1,1,1-trichloro- 160 C3H3C130 000918-00-3 64 2 4-Penten-2-one 84 C5H80 013891-87-7 9 3 Ethanol,/2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 4 1-Acetoxy-2-(dodecyloxy)ethane 272 C16H32O3 000000-00-0 9 Abundance Scan 277 (7.586 min): 31405.D (-) m/z 43.05 100.00% 4(3

5000

7.20 7.40 7.60 7.80 8.00

miz-? +49++6372+8288,.974103,117/14 — ' ■ i ■ • ■ ■ i • ■ ■ ■ i ■ 10 20 30 40 35 ‘*1 1 50 60 70 80 90 100 110 120 130 m/z 124.8 8.78% Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 7.20 7.40 7.60 7.80 8.00

A 15 m/z 46.85 6.11% 35 49 85 97 117 125 ‘ ' I ' * ’ ‘ I ‘ ‘ * I '44 ‘ I ' ‘ I ’ ‘ ‘ ' I ‘ ' I ' ‘ ‘ I THr miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #555: i-Penter-2-0ns 43 i 1 1 1 ' 7.20 7.40 7.60 7.80 8.00 5000 m/z 81.85 5.97% 15 : 1,27 53 69 ■ i ■ • ■ ‘ i ■ ■ ■ ■ i1 84 • i ■ ■ ■ ■ i ‘ ' i1 ■ ■ ■ i * ■ ■ ■ i ■ ■ ■1111 miz-s 10 20 30 40 50__ 60 70 80 90 100 110 120 130 Abundance #9118: Ethanol, 2,2,2-trichloro- A...... .. M . 31 7.20 7.40 7.60 7.80 8.00 m/z 126.90 5.72% 5000 49 77 113119 miz-> mmmm 10 20 30 40 50 60 70 PPP 80 84 97 90 100 110 120 130 • I * ■ ■ i i ‘ ' i 1 ‘ ' ' I ' ■ 7.20 7.40 _A I ‘ ‘ 7.60 ‘ I ' ‘ ‘ ' I ‘ 1 7.80 8.00

31405.D GCMS0103.M Thu Feb 07 09:14:30 2002 Page 2

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