GCMS analysis results for sample AD31405, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31405.D Vial: 11 Acq On : 16 Jan 2002 9:25 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 3.89 ug/1 997147 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3 -Dioxolane , 2-methyl- 88 C4H802 000497-26-7 9 2 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 3 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2I 004360-57-0 9 4 Pentane, 3 -methoxy- 102 C6H14O _________ 036839-67-5 9 Abundance Scan 262 (7.448 min): 31405.D (-) m/z 73.00 100.00% 73

5000 43 ’ I*’I**I**’’IU’I 7.20 7.40 7.60 7.80 । ;

miz-> ■ ■ • i ■

20 —44 87 103 . ... 40 60 80 100 120 140 160 180 200 220 240 260 280 T I ■ ' ‘ ' I ' ‘ ‘ ‘ I ' ‘ ‘ ‘ I 1 ‘ ' 1 1 1 m/z 43.00 33.27% Abundance #62902:1,3-Dioxolane, 2-methyl- 73

5000 43 i 7.20 7.40 7.60 7.80 i 58 m/z 45.00 12.03% 27 I 87 111 . 11 I'i i 1 i .III....... ... ..... miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #6203 Siland tramethyl- 73 T ‘ * * | * i' I . I * ‘ IVTT. I i ■ > 7.20 7.40 7.60 7.80 5000 m/z 41.05 11.43%

45 15 -n-p-r-n-j-r 59 188 miz-> 20 40 60 80 100 120 140 160 180 266' 220 240 260 280 'Abundance #40191: 1,3-Dioxolane, 2-pentadecyl- i ■ i t I i । i । 1 ■ > । । ■ TTTTT 73 7.20 7.40 7.60 7.80 m/z 71.00 6.96% 5000

43 57 86 99 256 283 1 1 1 1 1 T ' I"1 1 1 1 1 1 13 । ■ ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.20 7.40 7.60 7.80

31405.D GCMS0103.M Thu Feb 07 09:14:26 2002 Page 1

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