GCMS analysis summary, sample AD31403, Feb 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1502\31403.D Vial: 12 Acq On : 15 Jan 2002 9:43 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 3.78 ug/1 839182 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 262 (7.449 min): 31403.D (-) m/z 73.0.0 100.00% 73

5000 43 .................. 1 —.......... 87 103 7.20 7.40 7.60 7.80 38 | 50 55 .61 67, । , /tI*1*4)* —IIITr ■ ■ ‘ i ' ''1 '* i • ■ ■ ■ i • i ' m/z 43.05 32.81% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73

5000 43 1 1 i ■ i TEBBnBGrrTrr 7.20 7.40 7.60 7.80 58 m/z 45.05 12.03% . 27 87 ; । . P J. 11 rTf ‘‘ I ' ■ m/z-> 10 20 30 40 50 __ 60___ 70 80 90___ 100___ 110. Abundance #2542: ilane, ettamelt- 73

7.20 7.40 7.60 7.80 5000 m/z

45 15 53 59 88 T-I—GKOLR—I—Bn—F/r m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572:3-Pentanol, 3-methyl- T’r 73 7.20 7.40 7.60 7.80 m/z 71.00 6.81% 5000- 55 45 87 27 , | ■ • i ‘ 1 • 1 1 1 1 1 1 I1* 1 ' ' 1 1 ' 1 f ' ' Mg i 1 ■ • i 1 r‘ ‘ i ■ ' ■ ' i ■ ■ 1 • i ■ 11nB——TTTTTTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31403.D GCMS1126.M Mon Feb 04 15:11:28 2002 Page 1

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