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GCMS analysis results for sample AD31405, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31405 conducted on February 13, 2002.

NYC-WTC_000018373–000018384

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018382
OCR text

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\JAN1602\31405.D Vial: 11 Acq On : 16 Jan 2002 9:25 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Benzenesulfonamide, N,4-dimeth Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.16 0.33 ug/1 102002 Phenanthrene-dl0 24.77

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Benzenesulfonamide, N, 4-dimethyl- 185 C8H11NO2S 000640-61-9 58 2 Benzeneethanamine 121 C8H11N 000064-04-0 47 3 Benza .ehyde, 3-benzyloxy-2-fluoro- 260 C15H13FO3 000000-00-0 37 4 Benzene, l-methyl-2-nitroso- 121 C7H7NO 000611-23-4 27 Abundance ( Scan 1974 (23.165 min): 31405.D (-) m/z 91.00 100.00% 91

5000 43 57 71 185 m . ।1111 121 155

miz-> 20 . ■ ■ ■ Il 417, 40 60 a 80 . 108 ,| 100 120 139 1111 ■»»r ■ *1 • j ’ 140 a 1**‘I**‘*1+**‘I‘*‘*I****I** 160 180 I 200 220 240 260 22.80 23.00 23.20 23.40 m/z 57.00 30.18% Abundance #19121: Benzenesulfonamide, N,4-dimethyl- Ml Of > . । of. . /Vro 0,4 5000 22.80 23.00 23.20 23.40 65 155 185 m/z 43.00 27.50% 30 121 48 ' i, ■ 108 | 139 ■ ‘ i ‘ • i 1 ■ ■ ■ i ■ ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance 464004; Bnzmnetat ardi 0 30

22.80 23.00 23.20 23.40 ' 5000 91 m/z 64.95 25.14% 65 77 121 104 *pn/2*1—m90‘t71113*‘111111*13—1m/111-—03133 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #35873: Benzaldehyde, 3-benzyioxy-2-fluoro-4-methoxy- * • i • 91 22.80 23.00 23.20 23.40 m/z 92.00 19.33% 5000 65 51I l t • ‘ I ‘ .77. _________________________________ 233 260 ‘11/n0//n//1/n///0/—/00/0/n////0///0/01/B/n ' r I • 111T1 11 1 1 1 1 ...... A....... miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 22.80 23.00 23.20 23.40

31405.D GCMS0103.M Thu Feb 07 09:14:35 2002 Page 3

NYC-WTC_000018382

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NYC-WTC_000018382Source: NYC Law Department, mirrored locally

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