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GCMS analysis results for sample AD26206, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26206 with unidentified compounds detected.

NYC-WTC_000031171–000031186

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26207.D Vial: 54 Acq On : 30 NOV 2001 6:37 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzenesulfonamide, N-butyl-N, Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 30.43 21.80 ug/1 4817500 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzenesulfonamide, N-butyl-N,4-dim 241 C12H19NO2S 010285-91-3 50 2 Benzenesulfonamide, N, 4-dimethyl-N- 241 C12H19NO2S 057186-71-7 38 3 Benzenesulfonamide, N, 4-dimethyl-N- 227 C11H17NO2S 057186-69-3 37 4 2-Phenyl-4-/Ccyanomethyl) -5-methyl-l 198 C11H10N4 013322-20-8 27 Abundance Scan 2765 (30.431 min): 26207.D (-) m/z 154.95 100.00% 91 155 198

5000 ) 45 65 _ 30.20 30.40 30.60 30.80 , —-77 1.126118.139 1 166 185 200 4,212 [ 228 242,255, . m/z 197.95 91.16% m/z-> 40 60 80 220 240 260 100 120 140 160 180 Abundance #32133: Benzenesulfonamide, N-butyl-N,4-dimethyl- 91 155 198

) V 5000 30.20 30*40 30.60 30.80 m/ z 91.00 88.21% 65 । 241 1 1 1 1 • ' । I 1 1 1 1 I 1 1 1 1 T 1 1 1 ‘ l ' ‘ ' i ‘ ‘ I ’ • • • l • • • • I • ' ' ' I ’ • ’ • I ’ ‘ ’ i ' miz->_____ 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #32134: Benzenesulfonamide, N,4-dimethyl-N-(2-methy!propyl)- 91 155 198

30.20 30.40 30.60 30.80 m/z 146.10 29.95% 5000 65 2 mz->_____ 40 ... 60 8b 100 120 140 160 180 200 220 240 260 241

Abundance #29317: Benzenesulfonamide, N,4-dimethyl-N-propyl- 91 155 198 30.20 30.40 30.60 30.80 m/z44.90 22.90%

5000

65 42 1 1 227 . . , 1 , . , . 1 1 .

m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 30.20 30.40 30.60 30.80

26207.D NP112601.M Mon Dec 03 13:11:09 2001 Page 7

NYC-WTC_000031185

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NYC-WTC_000031185Source: NYC Law Department, mirrored locally

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