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GCMS analysis results for sample AD26206, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26206 with unidentified compounds detected.

NYC-WTC_000031171–000031186

Folder label: “GCMS X 11/2/01 A 12/1/01”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \HPCHEM\1\DATA\NOV3001\26207 .D vial: 54 Acq On : 30 Nov 2001 6:37 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise : Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1-Propanamine, 3-methoxy- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 28.84 18.61 ug/1 5337030 Phenanthrene-dl0 25.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Propanamine, 3-methoxy- 89 C4H11NO 005332-73-0 35 2 2,4-Diethy^5-methylthiazole 155 C8H13NS 052414-89-8 27 3 Benzene, -[(2-chloroethyl)sulfonyl 218 C9H11C1O2S 022381-53-9 23 42-(Propy mino)ethanol 103 C5H13NO 016369-21-4 14 Abundance Scan 2592 (28.843 min): 26207.D (■) m/z 91.00 100.00% si 72 155 45 59 5000 199 J L 28.60 28.80 29.00 29.20

miz—> 20 —l - 60 40 — 80 100 103116 —139 41186 130 ; , 216229 244173.. 288 T TIrr--1t‘‘111r T ‘I 1’11111 ■ 120 140 160 180 200 ZS) 240 260 280 m/z 72.00 81.10% Abundance #882:1-Propanamine, 3-methoxy- 33

- 5000 72 28*60 28.80 29.00 29.20 45 m/z 154.90 71.63% PTTmr 50.189 ................................... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #67210: 2,4-Diethyl-5-methylthiazole 140 ite —PP ---PP 28.60 28.80 29.00 29.20 59 100 m/ Z 45.00 52.36% 5000 45

71 85 127 8 : t : I j : i i : । i : : : | : » : : | : ) i 1TIIsT5-11131 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #27044: Benzene, 1-[(2-chloroethyl)sulfonyl4-methyl- B.B i : 7 1 i i /i i ] i 1T 1T I I I J : I i SI 28.60 28.80 29.00 29.20 155 m/z 59.05 48.82%

5000 218 139 190 .............. ,197 ..■Ji....... — 1 I " "1 1 " 1 I " m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 28.60 28.80 29.00 29.20

26207.D NP112601.M Mon Dec 03 13:11:07 2001 Page 6

NYC-WTC_000031184

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NYC-WTC_000031184Source: NYC Law Department, mirrored locally

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Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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