NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30357.D Vial: 18
Acq On : 28 Dec 2001 4:40 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 8 Benzeneethanamine, N-[(pentafl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
22.79 2.76 ug/1 1258690 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37
2 N-(Trifluoracetyl)-0,0’,0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37
3 N-(Trifluoroacetyl)-0,0',O''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37
4 N-(Trifluoroacetyl)-N,O,Q*,0*'-tetr 553 C22H42F3NO4Si4 000000-00-0 35
Abundance Scan 1933 (22.787 min): 30357.D (-) m/ z 73.0,0 100.00%
73
5000
147 355
221
45
— —**
117 191,
191, Tr 249
281 I
J, 3^ J, , 401 . ....550 22.40 22.60 22.80 23.00 23.20
m/z 147.00 2 6.59%
miz-> 50 100 150 200 250 300 ' 350 400 450 500
Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene]
73 355
5000
22.40 22.60 22.80 23.00 23.20
45
m/z 355.05 24.32%
| 208 251 281 , 386 458 548
‘ I‘ ‘I‘+‘*)+**I***1***‘I****I “i—i • I i T ■ ■ । ■ i ■ ■ • ■ i ■ ■
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58807; N-(Trifluoracetyn)-0,C.0"tris(trimethylsilyl)epin
73
355 • i J • • • i ' i ' 1 1 1 I ' 1
22.40 22.60 22.80 23.00 23.20
5000 m/z 221.05 18.35%
45
140 184 281 1 480
TT 1 ‘ i ■ • ‘ ■ i 1 ' ‘ • i • ■ ■ 1 i ' ' ■ • i 1 ■ • ■ i ' ■ 1 1 i ‘ ‘ i ■ ■
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no
73 22.40 22.60 22.80 23.00 23.20
355 m/z 281.00 13.84%
5000
45
— 120147 193 265 481
m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30357.D GCMS1126.M Wed Jan 02 11:00:31 2002 Page 8
NYC-WTC_000017762
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