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GCMS analysis results for sample AD30357, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.

NYC-WTC_000017748–000017769

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30357.D Vial: 18 Acq On : 28 Dec 2001 4:40 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

26.89 1.54 ug/1 703785 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 36 4 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35 Abundance Scan 2380 (26.891 mln): ' 30357.D (-)‘ m/z 73.00 1 00.00% 73

5000 147 221 281 249 [ 327 355 401 *29 26.60 26.80 27.00 27.20 45 TH dnlHa ore 117 1914. —L 250 m/z 147.0,0 32.22% miz-> 50 100 150 200 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 ■ • • i ■ ■ ■ ■ i r 1 ■ 11 ‘ ‘ i ■ ■ •1 5000 281 26.60 26.80 27.00 27.20 45 ■ 369 m/z 281.00 17.77% | , 117 207 249 • ■■i ■ ■ ■ • i ■ • 1 ■ 1 1 TTInnom 1 i • 1 1 1 t ■ ’1 1r1111i'■■■i■‘■• i • • m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-Isopropoxy-1.1.1.4,6.7-hexamethyl-3,5,5-tris(trim 73 . ........ M........... 26.60 26.80 27.00 27.20 5000 m/z 221.05 16.08% 147 221 281 327 3 519 561 415 । । । । । mrit । । > '| । । । । । >7 IIl*)*** miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethyisilyl ether 73 26.60 26.80 27.00 27.20 m/z 207.00 7.86% 207 5000 147 34 103 281 395 11 , 482 T*11r2*31*1 —***—**-*-T16*319T ■ 1 i ■ 1 —ITPfrTro m/z-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20

30357.D GCMS1126.M Wed Jan 02 11:00:35 2002 Page 9

NYC-WTC_000017763

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NYC-WTC_000017763Source: NYC Law Department, mirrored locally

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