NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30357.D Vial: 18
Acq On : 28 Dec 2001 4:40 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
26.89 1.54 ug/1 703785 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42
2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 36
4 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35
Abundance Scan 2380 (26.891 mln):
' 30357.D (-)‘ m/z 73.00 1 00.00%
73
5000
147
221 281
249 [ 327 355 401 *29 26.60 26.80 27.00 27.20
45
TH dnlHa ore
117
1914. —L 250 m/z 147.0,0 32.22%
miz-> 50 100 150 200 300 350 400 450 500 550
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73
147
■ • • i ■ ■ ■ ■ i r 1 ■ 11 ‘ ‘ i ■ ■ •1
5000
281 26.60 26.80 27.00 27.20
45 ■ 369 m/z 281.00 17.77%
| , 117 207 249
• ■■i ■ ■ ■ • i ■ • 1 ■ 1 1 TTInnom 1 i • 1 1 1 t ■ ’1 1r1111i'■■■i■‘■• i • •
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503; 3-Isopropoxy-1.1.1.4,6.7-hexamethyl-3,5,5-tris(trim
73
. ........ M...........
26.60 26.80 27.00 27.20
5000 m/z 221.05 16.08%
147
221 281 327 3
519 561 415
। । । । । mrit । । > '| । । । । । >7 IIl*)***
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871:1-Monolinoleoylglycerol trimethyisilyl ether
73 26.60 26.80 27.00 27.20
m/z 207.00 7.86%
207
5000 147
34 103 281
395
11 , 482
T*11r2*31*1 —***—**-*-T16*319T ■ 1 i ■ 1 —ITPfrTro
m/z-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20
30357.D GCMS1126.M Wed Jan 02 11:00:35 2002 Page 9
NYC-WTC_000017763
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