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GCMS analysis results for sample AD27288, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.

NYC-WTC_000018005–000018025

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01

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Scanned page image, NYC-WTC_000018020
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

26.74 0.72 ug/1 247376 Phenanthrene-dl0 24.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1.1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 59 2 3-Isopropoxy-Xj l,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28 4 1,1,1,5,7, ,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 Abundance 2 Scan 2363 (26.740 mln): 27288.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 - 26.40 26.60 26.80 27.00 n re, ., 1914 1.249 . | 325,355, 401.429 45 TT 5 । 117 m/z 147.00 33.96% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 26.40 26.60 26.80 27.00 ' 369 m/z 281.00 19.12% 1 338 | 207 249, ——— - ■ i • • ■ ■ i ■ 1 ■ ■ i • ■ * ■ i • • • • i • • ■ • i ■ • m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503. 3-Isopropoxy-1,1.1.7,7,7-hexamethyl-3,5,5-tris(trim 73 ....................................... ..... 26.40 26.60 26.80 27.00 5000 m/z 221.05 17.11% 147 221 281 327 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether i 73 26.40 26.60 26.80 27.00 m/z 207.00 8.59% 207 5000 147 34 103 281

m/z-> -------------------- 50 100 150 200 250 300 350 +3242 400450500550 .......... M............ 26.40 26.60 26.80 27.00

27288.D GCMS0103.M Thu Jan 10 09:37:07 2002 Page 8

NYC-WTC_000018020

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NYC-WTC_000018020Source: NYC Law Department, mirrored locally

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