NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26
Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS
Sample gems scan 12/20a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
26.74 0.72 ug/1 247376 Phenanthrene-dl0 24.80
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1.1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 59
2 3-Isopropoxy-Xj l,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28
4 1,1,1,5,7, ,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16
Abundance 2 Scan 2363 (26.740 mln): 27288.D (-) m/ z 73.00 100.00%
73
5000
147
221 281 -
26.40 26.60 26.80 27.00
n re, ., 1914 1.249 . | 325,355, 401.429
45
TT 5 । 117 m/z 147.00 33.96%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147
281
5000
26.40 26.60 26.80 27.00 '
369 m/z 281.00 19.12%
1
338 | 207 249,
——— - ■ i • • ■ ■ i ■ 1 ■ ■ i • ■ * ■ i • • • • i • • ■ • i ■ •
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503. 3-Isopropoxy-1,1.1.7,7,7-hexamethyl-3,5,5-tris(trim
73
....................................... .....
26.40 26.60 26.80 27.00
5000 m/z 221.05 17.11%
147
221 281 327 415 519 561
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
i 73 26.40 26.60 26.80 27.00
m/z 207.00 8.59%
207
5000 147
34 103 281
m/z->
--------------------
50 100 150 200 250 300 350
+3242
400450500550
.......... M............
26.40 26.60 26.80 27.00
27288.D GCMS0103.M Thu Jan 10 09:37:07 2002 Page 8
NYC-WTC_000018020
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