NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30933.D Vial: 50
Acq On 2 Jan 2002 2:22 pm Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
28.65 0.25 ug/1 75970 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1/i,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38
3 Trisiloxane,/ 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 25
4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 10
Abundance Scan 2572 (28.654 mln): 30933.D (-) m/ z 73.00 1 00.00%
73
5000
147
221 281 355 ■ i • • 1"1 i 11 1 '
45 117 325, | .429 28.40 28.60 28.80 29.00
m/z->
1 ■•n > r ■ ■ i ■
50 100
^4. .1914 *’1**814
150 200 250 300 350 400 450 500 550
m/z 147.00 37.21%
Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
5000 ’*1**1*’’’1’**I*
147 28.40 28.60 28.80 29.00
221 231 327
m/z 221.05 20.99%
415 519 561
L
■ • t ■ ‘ ■ i ‘ ‘ i ' »
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
i 73
207
L
28.40 28.60 28.80 29.00
5000 147 m/z 355.0 17.91%
34 103
281
395
A
TT1d1tt1-1*’111*11111-11--uu
482
—m———*T0IIII71111T
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147 28.40 28.60 28'80 29.00
281
m/z 281.0,0 17.31%
5000
369
207 249,
I
miz->
• 1 i • 1 1 ■ i ■ ■
50 100 150
meltih..J r338
200
.................................
‘ | ‘ 11 "T T 1 1 I * r i
250 300 350
pi i t i । i j t i । j j
400
j
450 500 550 28.40 28.60 28.80 29.00
30933.D GCMS1126.M Fri Jan 25 11:43:45 2002 Page 8
NYC-WTC_000018730
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