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GC/MS analysis results for sample AD30933, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.

NYC-WTC_000018716–000018732

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30933.D Vial: 50 Acq On 2 Jan 2002 2:22 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 28.65 0.25 ug/1 75970 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1/i,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 Trisiloxane,/ 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 25 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 10 Abundance Scan 2572 (28.654 mln): 30933.D (-) m/ z 73.00 1 00.00% 73

5000 147 221 281 355 ■ i • • 1"1 i 11 1 ' 45 117 325, | .429 28.40 28.60 28.80 29.00

m/z-> 1 ■•n > r ■ ■ i ■ 50 100 ^4. .1914 *’1**814 150 200 250 300 350 400 450 500 550 m/z 147.00 37.21% Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ’*1**1*’’’1’**I* 147 28.40 28.60 28.80 29.00 221 231 327 m/z 221.05 20.99% 415 519 561 L ■ • t ■ ‘ ■ i ‘ ‘ i ' » m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether i 73

207 L 28.40 28.60 28.80 29.00 5000 147 m/z 355.0 17.91% 34 103 281 395 A TT1d1tt1-1*’111*11111-11--uu 482 —m———*T0IIII71111T miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 28.40 28.60 28'80 29.00 281 m/z 281.0,0 17.31% 5000

369 207 249, I miz-> • 1 i • 1 1 ■ i ■ ■ 50 100 150 meltih..J r338 200 ................................. ‘ | ‘ 11 "T T 1 1 I * r i 250 300 350 pi i t i । i j t i । j j 400 j 450 500 550 28.40 28.60 28.80 29.00

30933.D GCMS1126.M Fri Jan 25 11:43:45 2002 Page 8

NYC-WTC_000018730

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NYC-WTC_000018730Source: NYC Law Department, mirrored locally

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