Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
NYC-WTC_000018716–000018732Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30933.D Vial: 50 Acq On 2 Jan 2002 2:22 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
26.89 0.32 ug/1 98199 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207S17 071579-69-6 38 2 Butanoic acid, 3-methyl-3-[(trimeth 262 CllH26O3Si2 055124-90-8 32 3 trans-3-Hexenedioic acid, bis(trime 288 C12H24O4S12 000000-00-0 23 4 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 Abundance Scan 2380 (26.892 mln): 30933.D (-) m/z 73.0,0 100.00% 73
5000 147 221 281 ‘ 11* 11 ■ IFTI ■ 26.60 26.80 27.00 27.20 ’r 1 ■' TITt . 1911 1,249.1, . —I"I——mOmRUmTT 45 117 327 355 429 m/z 147.00 31.00% m&~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
..... /. 5000 147 26.60 26.80 27.00 27.20 221 281 m/z 281.00 16.74% 327 415 519 561 — 11114* miz-> ’50 100 150 200 250 300 350 400 450 500 550 Abundance 436157 Butanoic acid. 3-methyl-3-[(trimethylsilyl)oxyH, t 73 131 T T T TB.T 26.60 26.80 27,00 27.20 5000 m/z 221.05 15.57% 247 47 205 | m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40770: trans-3-Hexenedioic acid, bis(trimethylsily) ester 73 26.60 26.80 27.00 27.20 m/z 74.00 9.44% 5000 147 45 | 112 244 273 i______________________________________________ ' 1 h—i — __________ i 1 1 I 1 1 1 1 I 1 1 ' 1 i ' ' ' 1 i ■ ■ ' ■ i ' 1 ' ‘ i • ' ■ ■ i 1 ' • ‘ i ■ • miz-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20
30933.D GCMS1126.M Fri Jan 25 11:43:40 2002 Page 7
NYC-WTC_000018729
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NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
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