NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30605.D Vial: 30
Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
28.66 0.30 ug/1 102614 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 37
2 1-Monolin eoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 33
3 Trisiloxa.ne, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25
4 Benzoic” acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 17
Abundance Scan 2572 (28.658 mln): 30605.D (-) m/z 73.00 1 00.00%
73
5000
147
221 281 355
45 117 , 191 [,249 [ :325 [ 401 429 ........... . , . 28.40 28.60 28.80 29.00
TT —me । f । r । It ii r > । i m/z 147.00 33.93%
m/z-> 50 100 150 200 250 300i 350 400 450 500 550
Abundance #60503:3-Isopropoxy-1,1,1,7>7,7-hexamethyl-3,5,5-tris(trim
73
5000 T
1 \
I ’1* I
147 28.40 28.60 28.80 29.00
221 281 327 m/z 355.05 21.42%
415 519 561
L ,
•*I**‘*I‘‘**I*‘**}****I‘**I********1*** ‘1****I I"r ■n 'r
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871:1-Monolinoleoyiglycerol trimethylsilyl ether
73
207 28.40 28.60 28.80 29.00
5000 147 m/z 221.05 19.18%
34 103 281
395 482
* * । * ' * » t • * ■ 1 i 1 ■ ■ ■ i ' ‘ ' i ‘ ‘ ■ i ‘ ■ i ■ • • ■ i ■ ' ■ ' i ' '
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet T
) V
i ‘ '
T-r-r-r-n-r-r
73 147 28.40 28.60 28.80 29.00
281
m/z 281.00 17.62%
i 5000
369
207 249, 338 I............ ................
I 1 ' I ' 1 1 PI 1 unni tih
miz-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00
30605.D GCMS1126.M Wed Jan 23 08:29:15 2002 Page 10
NYC-WTC_000018210
OCR can misread numbers and units. Confirm readings against the page image before using them.