NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39
Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
28.65 1.50 ug/1 612351 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1 -Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36
2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32
3 3-Isoprp^oxy-l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25
4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 25
■Abundance Scan 2572 (28.654 min): 30985.D (-) m/ z 73.0,0 100.00%
73
5000
147
221 281 355 ■ ■ ■ ■ ।'1' • f • •1 • ।i । ■
, 191/ 1 249., 1 . 327. | 401 429 28.40 28.60 28.80 29.00
45 117
■ 13 1 IB*" j i PT tt i j 14 Fih —= n i j j t i i i—।—i—r m/z 147.00 34.64%
mlz~> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871:1-Monollnoleoylglycerol trimethylsilyl ether
73
207
5000 147 II**I****I*IT 1 i • • • ■ । ■
28.40 28.60 28.80 29.00
34 103 ! 281 m/z 221.05 19.90%
325 482
m/z-> 50 100 150 200 250 ‘ 300 350 400 450 500 550
Abundance #52459; Trisiloxane, 1,1.1 5.5.5-hexamethyl-3.3-bisi(trimet
73 147
281 28.40 28.60 28.80 29.00
5000 m/z 355.05 18.91%
369
207 249
' i ■ ‘ ' i ■ ' ‘ ' i • ■ ■ • i 1 ■ ■ ' I ‘
338 ,..................
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim /_________
■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ’ i ■ ■
73 28.40 28.60 28.80 29.00
m/z 281.00 14.44%
A.
5000
147
221 281
327 . 415, . ...... 519.561 -----
m/z-> 50 100 150 200 250 300 350 400 450 500 550 ′ 28.40 28.60 28.80 29.00
30985.D GCMS1126.M Wed Jan 23 08:57:46 2002 Page 10
NYC-WTC_000018278
OCR can misread numbers and units. Confirm readings against the page image before using them.