Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
NYC-WTC_000018174–000018193Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30714.D Vial: 29 Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
28.65 0.45 ug/1 166512 Phenanthrene-dl0 24.98
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 33 2 3-1sopropoxy-1, ,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 30 3 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604S15 003555-47-3 27 4 Benzoic acid , 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 25 Abundance A Scan 2572 (28.655 mln): 30714.D (-) m/z 73.0,0 100.00% 73
5000 147 221 281 355 1 28.40 28.60 28.80 29.00 i • • ‘H ' 1 45 117 191 1 249 l . 325. [ 401 429 —THt daa/H/m0 r,'| . . i ........................... । . . . . [ i . j । . m/z 147.00 33.51% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73
207 5000 147 I 28.40 28*60 28*80 29.00 34 103 ! m/z 221.05 18.76%
m/z-> Abundance 50 100 150 200 ..7250 300 350 400 450 500 395 1 ,
#60503: 3-Isopropoxy1,1.1 ./.7.7-hexamethyl-3,5,5-trs(trim 482 550 73 1J**** 28.40 28.60 28.80 29.00 5000 m/z 355.05 16.96% 147 221 281 327 415 519 561 ’m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet ) 1 73 147 28.40 28.60 28.80 29.00 281 m/z 281.00 14.60% 5000
369 , 338 I_______________ 207 249, —2/7 114*1**1 ‘ ‘ i ‘ ‘ I ■ ' ‘ ‘ l ‘ 1 ' ' l 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00
30714.D GCMS1126.M Wed Jan 23 08:50:29 2002 Page 9
NYC-WTC_000018189
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NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder