NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39
Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
26.89 1.90 ug/1 774406 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinol >ylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36
2 Trisiloxa: , 1,1,1,5,5,5-hexamethyl 384 C12H3604S15 003555-47-3 36
3 1,1,1,5,,7,7-Heptamethy1-3,3-bis (t 444 C13H40O5S16 038147-00-1 35
4 3-ISO] opoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25
Abundance Scan 2380 (26.891 min): 30985.D (-) m/ z 73.00 100.00%
73
5000
147
221 281 111 ■ ‘4 ■ ।r ■ ■11 ■ ■ ‘ । ■
45 . 96 117 s 191 L 251 [ 327,325 401 429 26.60 26.80 27.00 27.20
i , ■ ‘ ’i 1 ' Mi* । ■ i *1* A. ■ Ti* Fi* ■ r |k. । ■■■■ T i-. » । ■ । ■ । ■ m/z 147.00 33.84%
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147
26.60 26.80 27.00 27.20
34 103 m/z 281.00 18.98%
I
m/z-> 50 100 150 200
1.A 250 300 350 400 450
482
Abundance 452459: Trisiloxane, 1.1.1 5.5,5-hexamethyl-3.3-bis(trimet
73 147
■ ■ ■ । ■ ■ ■ ■ । i • ■ ■ ' । ■
281 26.60 26.80 27.00 27.20
5000 m/z 221.05 16.10%
207 369
1 ; 249 A. 338 i
— **111444/1*
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t T-r-j-r-r ' ' I ‘ ‘
73 26.60 26.80 27.00 27.20
m/z 74.0.0 8.02%
147
5000 267
355 429
207
m/z->
I.....
45
50 100 150
• ■
200
i
I I ■ ■ ■ •
250
i ■ ■
....91
300 350
■ ■
400
i ■ ■ 1
450
r1 1
11./.......... .
26.60 26.80 27.00 27.20
30985.D GCMS1126.M Wed Jan 23 08:57:40 2002 Page 9
NYC-WTC_000018277
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