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GCMS analysis results for sample AD30985, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

26.89 1.90 ug/1 774406 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinol >ylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36 2 Trisiloxa: , 1,1,1,5,5,5-hexamethyl 384 C12H3604S15 003555-47-3 36 3 1,1,1,5,,7,7-Heptamethy1-3,3-bis (t 444 C13H40O5S16 038147-00-1 35 4 3-ISO] opoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 Abundance Scan 2380 (26.891 min): 30985.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 111 ■ ‘4 ■ ।r ■ ■11 ■ ■ ‘ । ■ 45 . 96 117 s 191 L 251 [ 327,325 401 429 26.60 26.80 27.00 27.20 i , ■ ‘ ’i 1 ' Mi* । ■ i *1* A. ■ Ti* Fi* ■ r |k. । ■■■■ T i-. » । ■ । ■ । ■ m/z 147.00 33.84% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 26.60 26.80 27.00 27.20 34 103 m/z 281.00 18.98% I m/z-> 50 100 150 200 1.A 250 300 350 400 450 482

Abundance 452459: Trisiloxane, 1.1.1 5.5,5-hexamethyl-3.3-bis(trimet 73 147 ■ ■ ■ । ■ ■ ■ ■ । i • ■ ■ ' । ■ 281 26.60 26.80 27.00 27.20 5000 m/z 221.05 16.10%

207 369 1 ; 249 A. 338 i — **111444/1* m/z-> 50 100 150 200 250 300 350 400 450 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t T-r-j-r-r ' ' I ‘ ‘ 73 26.60 26.80 27.00 27.20 m/z 74.0.0 8.02% 147 5000 267 355 429 207

m/z-> I..... 45

50 100 150 • ■

200 i I I ■ ■ ■ •

250 i ■ ■ ....91 300 350 ■ ■ 400 i ■ ■ 1 450 r1 1 11./.......... . 26.60 26.80 27.00 27.20

30985.D GCMS1126.M Wed Jan 23 08:57:40 2002 Page 9

NYC-WTC_000018277

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NYC-WTC_000018277Source: NYC Law Department, mirrored locally

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