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GCMS analysis results for sample AD30985, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Benzeneethanamine, N-[(pentafl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.79 3.89 ug/1 1586800 Phenanthrene-dl0 24.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 N- (Trifluoroacetyl) -0,0’,0’'-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 3 N-(Trifluoroacetyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 27 4 Benz c acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 25 Abundance Scan 1933 (22.787 mln): 30985.D (-) m/z 73.0,0 100.00% 73

5000 147 355 221 281 ' T' 11414 * 1"I‘4 r1'1 T 1 1 401 443 327 [ f 45 04 J 117, ,4., 191, [ 249, I tFi IFah Pair 14 rtau Fih i i i ■ i । ■ i , t-, r t 22.40 22.60 22.80 23.00 23.20 m/z 147.00 25.20% miz-> 50 100 150 200 250 300 350 400 450 500 550 [Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene] 73 355

5000 I | f I I J J 5 I 'I J r T I I J" I 1' 11 '! J ! I 22.40 22.60 22.80 23.00 23.20 45 m/z 355.0 23.16% 208 251 281 386 458 548 ■ 1 i • • • ■ i ■ • 1 ■ i • ‘ ■ ■ i ■ • ' ■ i 1 T—YT । > ""’SITUT" । . . ll । i । , । > m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluproacety!)-O.0‘,0"-tris(trimethylsilyl)no 73 355 • i * * * • i '* ‘ • * r 176" r * * * 1 i ′′ 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 17.68%

45 !I 120147 193 265 | 481 miz-> ■ ■ I ■ ■ ■ ■ i • ‘ 50 100 ■ i ■ ■ 1 ■ i • • ■ ■ i 1 150 200 250 ‘ I ‘ ‘ ‘ • I 1 ' 1 ' I ■ ' ‘ ' I ' ' ‘ ‘ I ■ 1 11 1 1 1 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacety!)-N,O,0’,0"-tetrakis(trimethylsi TIT T T 1***111 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 13.27% 355 5000

45 fl 147 193 267 538 T*1/1/7/1/*2/"///*2///**n/—/"/"/"/I." 1141441144,4 tt**I*I* miz-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30985.D GCMS1126.M Wed Jan 23 08:57:35 2002 Page 8

NYC-WTC_000018276

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NYC-WTC_000018276Source: NYC Law Department, mirrored locally

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