Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
NYC-WTC_000018093–000018106Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30694.D Vial: 31 Acq On 1 Jan 2002 6:01 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzeneethanamine, N-[(pentafl Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
22.80 0.36 ug/1 111350 Phenanthrene-dl0 24.98
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 N- (Trifluoracetyl) -0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 Benzoic acid, 2,5-bis (trimethylsilo 370 C16H30O4S13 003618-20-0 38 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 32 Abundance Scan 1934 (22.797 min): 30694.D (-) m/z 73.00 100.00% 73
5000 147 355 221 281 401 22.40 22.60 22.80 23.00 23.20 45 117 249. | 327 t 1 1 t I । 191 TT11< । ■ . l m/z 147.00 26.40% m/z-? • 50 100 150 200 250 300 350 400 450 500 ’ 550 Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene] 73 355 %
5000 I 111 '1 ■ ' 1 rl T T 22.40 22.60 22.80 23.00 23.20 * 45 m/z 355.05 26.34% , | 208 251 281 386 458 548 TTTmnmn—n——amB—dm—mOmDTTTTTT 1II+III*T’t m/z-> 50 100 150 200 250 300 350 400, 450 500 550 Abundance #58807: N-(Trifluoracety)-0,0’.O"-tris(trimethylsilyl)epin 73 355 I • ‘ * I • ‘ 4 1 I T T 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 17.95%
45 140 184 281 480 ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ' ‘ • i ■ ' ■ • i 1 ‘ ‘ • I • ■ ■ • l ■ ‘ I 1 ' 1 ' 1 1 ''1 1 I ' i‘ 'T' . miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73978: Benzoic acid. 2,5-bis(trimethylsiloxy)-, trimethyls 73 22.40 22.60 22.80 23.00 23.20 355 m/z 281.00 14.39% 5000 45 | U7 179 223 267 297 1 1 I ‘ 1 1 1 1 1 1 ■'1 ! 1 1 11 1 1 '' 1 1 1 11 ( 1 1 1 ' r r T . i ■. i. ■ ■. j •. i • ।. । . m/z—> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30694.D GCMS1126.M Wed Jan 23 08:31:30.2002 Page 6
NYC-WTC_000018105
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NYC-WTC_000018142
Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018248
Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
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NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
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NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
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NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder