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GCMS analysis results for sample AD31075, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017478–000017493

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31075.D Vial: 11 Acq On 8 Jan 2002 11:06 pm Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzeneethanamine, N-[(pentafl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.74 ug/1 221317 Phenanthrene-dl0 24.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 46 2 N-(Trifluorpacetyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 43 3 N- (Trifluoracetyl) -0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 4 Benzoic acid. 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 Abundance / Scan 1916 (22.637 mln): 31075.D (-) 1 m/z 73.0.0 100.00%

5000 147 355 * 221 281 45 ■ I I ‘ 117. 19141 251, [ 327 I 401 22.40 22.60 22.80 23.00 m/z 147.00 26.19% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355

5000 22.40 22.60 22.80 23.00 m/z 355.05 21.62% 45 1 208 251 281 386 458 548 m/z->. 'sb ' 100 'l50 ’ 200 250 300 ’ 350 400 ’ 450 ' 500 550 Abundance ' I a/ tin 73

355 ... r22.40...22.60 /A..22.80 ........ 23.00 5000 m/z 221.05 17.90%

45 147 193 267 538 m/z-> 50__ 100 150 200 250 __ 300 .350 400 450 500 550 Abundance #58807: N-(Trifluoracetyij-b,O',O"-tris(trimethylsilyl)epin ‘ ’ 1 1 ‘ ‘ I ‘ ’ 713 22.40 22.60 22.80 23.00 355 m/z 281.10 13.92% 5000

45 I h 140 184 281 480 ‘ ‘ ’ l 1 ‘ ' I ‘ —HT ' 1 ‘ I ‘ ‘ ‘ ' I 1 ‘ ‘ * i ‘ ■ i ■ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00

31075.D GCMS0103.M Wed Jan 09 12:28:17 2002 Page 7

NYC-WTC_000017491

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NYC-WTC_000017491Source: NYC Law Department, mirrored locally

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