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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017424
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Benzeneethanamine, N-[(pentafl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.64 3.60 ug/1 1372480 Phenanthrene-dl0 24.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 38 4 N-(Trif oroacetyl)-N,0,0',0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 35 Abundance Scan 1917 (22.640 mln): 31074.D (-) m/z 72.95 100.00% 73

5000 147 355 221 281 | 22.40 22.60 22.80 23.00 — 45 117 7 191, L 249, I ■i "iti i r" / i 7f rh i" r—Tjmi 327 | 41 441........... . m/z 355.05 27.43% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyljmethylene] 73 355

5000 ’ * I ‘ ‘ * 4 I ' ' • * I ‘ ‘ 22.40 22.60 22.80 23.00 m/z 147.00 27.41% 45 | 208 251 281 386 458 548 m/z— 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 355 ■ ■ i ■ ■ 1 ‘'I''' '-"1“ 22.40 22.60 22.80 23.00 5000 m/z 221.05 18.45%

45 140 184 281 480 ■ ■ i ■ ' ■ ■ i • ■ ■ ■ i • • ■ 1 i ■ • ■ ■ i ■ ■ 1 ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■

m/z-> 50___ 100 150 200 250 300 350 400__ 450 500 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy>, trimethyls tttPt 73 22.40 22.60 22.80 23.00 355 m/z 281.00 14.80% 5000 45 ,147 179 223 267 297 4 4 ! 4 1 4 4 1 4 4 4 4 I 4 4 4 4 I 4 ‘ 4 4 I 4 4 ? 4 ! 4 4 4 ‘ I 4 ■ ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 4 4 1 4 4 4 4 I4 14 4 [1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00

31074.D GCMS0103.M Wed Jan 09 12:25:04 2002 Page 12

NYC-WTC_000017424

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NYC-WTC_000017424Source: NYC Law Department, mirrored locally

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