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GCMS analysis results for sample AD27288, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.

NYC-WTC_000018005–000018025

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01

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Scanned page image, NYC-WTC_000018019
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzeneethanamine, N-[(pentafl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.64 1.72 ug/1 590112 Phenanthrene-dl0 24.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Benzeneethar amine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 3 N-(Trifluoracetyl)-0,0',0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 4 N-(Tr/fluoroacetyl)-0,0',0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 Abundance Scan 1916 (22.636 min): 27288.D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 ■ ■ i ■ ■ ■ i ■ * * ‘ I ■ ■

- 191 401 22.40 22.60 22.80 23.00 45 117 249. [ 327- miz-? 0 h4- 50 100 150 200 250 । i T fi । i rti 300 350 400 450 500 550 ′ m/z 147.00 25.05% Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methyIene] 73 355

5000 1 ■ i 1 • • > i ■ • • • i > > 22.40 22.60 22.80 23.00 m/z 355.05 22.67% 45 208 251.281 386 458 548 ’ * 1 1 1 ‘ I * * ‘ • I • • * ’ I ‘ ‘ ‘ * /-"6T88 • । । * > * . j । । । । > l . » . » j i i m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459; Trisiloxane, 1,1,1,5.5,5-r<examethyi-3.3-bis[(Wmct 73 147 *‘I* 281 22.40 22.60 22.80 23.00 5000 m/z 221.05 17.29% 369 207 249 | 338 UOBBByBOBOBnBGITT m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O',O' ’-tris(trirnetfiylsilyl)epin -P - 73 22.40 22.60 22.80 23.00 355 m/z 281.00 13.47% 5000

45 1 , 140 184 281 480 * 1 1 * ’ 1 • 1 • r "4 ‘I ■ ' i ■ ■ ■ ■ i ■ • ■ • i • ■ 1 ■ i ■ ' 1 ‘ i ■ ■ ■ ■ i ■ ■ ------- m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00

27288.D GCMS0103.M Thu Jan 10 09:37:03 2002 Page 7

NYC-WTC_000018019

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NYC-WTC_000018019Source: NYC Law Department, mirrored locally

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