GCMS analysis summary, sample AD27288, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Benzeneethanamine, N-[(pentafl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.64 1.72 ug/1 590112 Phenanthrene- dl 0 24.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N- [(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 Trisiloxane, 1,1,1/5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 3 N-(Trifluoracetyl4-0,O1,O"-tris(tri 495 C20H36F3N04Si3 000000-00-0 37 4 N-(Trifluoroacet^l)-0,0',0»1-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 Abundance Scan 1916 (22.636 mln): 27288.D (-) m/z 73.00 100.00% 73

5000 .......... ................ ...................... 147 ,4 355 ■ 45 117 221 281 191, [ 249. 327 1I 401 22.40 22.60 22.80 23.00 0- ■ r+-r a**p m/z 147.00 2 5.05% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355

5000 ■ ■ i ■ • ■ • i • ■ ■ ■ i ‘ • 22.40 22.60 22.80 23.00 45 m/z 355.0 22.67% 208 251 281 386 458 548 ’ I***I***1**’*I*’**I4+’’I***I**’*}’’I’*+*I’* miz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance *32-09 T silosanc, ' 1.1 5Shoxamety-lsjtomd; 73 147 T T 281 22.40 22.60 22.80 23.00 5000 m/z 221.05 17.29% 369 207 249 ■ t i pn rn I f 338 l » » • i j t i i I | i i i i | । । 17 । m i I । 1.7 i I i I i I pi i I i j i j i I j i r m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O.O’,O"-tris(trimethylsilyl)epin • * i » • ■ ' r ■ ■ 1 ■ i ■ ■ 73 22.40 22.60 22.80 23.00 355 m/z 281.00 13.47% 5000

45 l k 140 184 281 480 ----- ' 1 I 1 11 1 1 1 ■ ’I’ ■ > 1 ‘ i • ■ ■ ' i 1 • ■ ■ i • ' ' ' i ' 1 ‘ 1 i • • ■ ■ i ■ 1 1 ■ I 1 11 * i ■ ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00

27288.D GCMS1126.M Mon Feb 04 15:23:22 2002 Page 8

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