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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017425
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

26.73 1.85 ug/1 707273 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 3 3-Isopro; oxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 4 1,1,1,3/ ,5,7,7,7-Nonamethyl-3-(tri 384 C12H3604Si5 038146-99-5 25 Abundance 7 73 Scan 2363 (26.734 min): 31074.D (-) m/z 73.00 100.00%

5000 147 221 281 45 1911 | 249 . [ 327,355 401 429 26.40 26.60 26.80 27.00 m/z-> 1 1 I’ 4 r 50 1-117814 100 r ............. TTfIRTmaumTTTTT 150 200 250 300 350 400 450 500 550 m/z 147.00 33.48% Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 26.40 26.60 26.80 27.00 34 103 m/z 281.00 281 17.78% - 3?5. ...482 ..... ... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance " ) nn me 1,1 - ■ c yis/ 1. :: , mo 73 147 281 26.40 26.60 26.80 27.00 5000 m/z 221.05 15.86% 369 207 249 338 m/z-> ' 50 ‘ wo ' iso " 200 ' 1 250 ‘ 300 ' ' 350 ' ‘ 400 ' ' 450 ‘ ' 500 ‘ ‘ 550 ' Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-Ms(trim 73 26.40 26.60 26.80 27.00 ' m/z 74.00 8.52% 5000 147 221 281 39 415 [ I i7 1 519 561 - m/z~> 50 100 150 200 250 300 350 400 450 500 550 26.40 26.60 26.80 27.00

31074.D GCMS0103.M Wed Jan 09 12:25:09 2002 Page 13

NYC-WTC_000017425

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NYC-WTC_000017425Source: NYC Law Department, mirrored locally

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