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GCMS analysis log for sample AD30714, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.

NYC-WTC_000018174–000018193

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018188
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\30714.D Vial: 29 Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 1-Monolinoleoylglycerol trimet Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.89 0.64 ug/1 234640 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 4 4-Cyclohexene-1,2-dicarboxylic acid 348 C14H25ClO4Si2 106450-29-7 23 Abundance Scan 2380 (26.892 mln): 30714.D (-) m/ z 73.0,0 100.00% 73

5000 147 221 281 26.60 26.80 27.00 27.20 45 117 191 [ 249 ( 325,355 399 429 • "I 1 ■ PI —fi 1rn/n/m//*m1s ........................... ‘—13*I‘1535318T m/z 147.00 32.33% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 — —. — 5000 147 T T 26.60 26.80 27.00 27.20 34 103 : m/z 221.05 15.86% 281 395 Zl J ' ‘ _L ‘ J ‘ 1 f • I * ' ’ ' t ‘ i . ‘ * I 482_______ ’ k I r' 1 ' 1 ‘ ‘ ' 1 ’ * m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance +52459 T rig’loxane, 1.1.1 5.5,5-hexamethyl-3.3-bis[(trimet 73 147 21 281 26.60 26.80 27.00 27'20 5000 m/z 281.00 15.47% 369 207 249 .338).. miz-> ‘50 100 150 200 250 ′ 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim IAIAPPOTT 73 26.60 26.80 27.00 27.20 m/z 74.00 8.67% 5000 147 221 T 327, 415 i r r । i rh r । i r 4 r । r "I II r i |-i IIrI 519 561 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20

30714.D GCMS1126.M Wed Jan 23 08:50:24 2002 Page 8

NYC-WTC_000018188

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NYC-WTC_000018188Source: NYC Law Department, mirrored locally

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