Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
NYC-WTC_000018174–000018193Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30714.D Vial: 29 Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 N-(Trifluoracetyl)-0,0’,O"-tri Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
22.79 1.49 ug/1 547252 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID • MW MolForm CAS# Qual
1 N- (Trifluoracety])-0,0’,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 2 N- (Trifluoroacetyl) -N,O,O' ,0”-tetr 553 C22H42F3NO4Si4 000000-00-0 43 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 4 N-(Triflu^roacetyl)-0,O»,O'1-tris(t 481 C19H34F3NO4S13 000000-00-0 37 Abundance Scan 1933 (22.789 min): 30714.D (-) m/z 73.00 100.00% 73
5000 147 221 281 355 ‘ | ‘ ‘ ‘ | ‘ | T 1 1 i t i » t t । ' i
45 .. 117 191. 249 [ 327 [ 401 22.40 22.60 22.80 23.00 23.20 I 1 ' 1 • i • 1 Pin 11* +**/lii Pi । ■ .-5 t 1 m/z 147.00 26.13% t I * miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracety)-o,O‘,0"-tris(trimethylsilyl)epin 73 355 5000 ' 1 ■ • • 1 1 1 ■ 1' l 1 ■ 1 1 1 • ■ 1 ■ 1 22.40 22.60 22.80 23.00 23.20 m/Z 355.05 21.25% 45 140 184 281 ...... ..... 40 * • i ■ • ■ ■ i • • ‘ • i 1 —**PITTTT i ' • ' 1 i ■ ' ‘ 1 i • ‘ ‘ i ■ ■ 1 • i ■ • • ■ i ' ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Triflucroacetyl)-N,O.O‘,0"-tetrakis(trimethylsi s 73 m.......... 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.0 16.52%
45 267 147 193 538 • • i 1 • ' • i 1 ■ ■ ■ i ■ ■ 1 • i ■ ■ ■ ■ i ' ■ 1 ‘ i ■ ‘ ' * 1 1 ■ ■ ■ 1 ■ ■ ■ 1 1 ■ ' • 1 1 ‘ ■ i • ' miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 22.40 22.60 22'80 23.00 23.20 m/z 281.00 13.41% 5000
45 208 251 281 386 458 548 ' 1 rr 1 T11——————TTT -r-r-j-r-r-r-r-p- Iactru - 1 ‘1 1,14 1P 1 1 1 1 romm miz-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30714.D GCMS1126.M Wed Jan 23 08:50:19 2002 Page 7
NYC-WTC_000018187
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NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder