Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
NYC-WTC_000018754–000018774Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30935.D Vial: 48 Acq On 2 Jan 2002 11:27 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 N-(Trifluoroacetyl)-0,0',0''-t Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.79 1.43 ug/1 515651 Phenanthrene-dl0 24.98
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 N- (Trifluoroacetyl) -0,0' ,0' '-tris (t 481 C19H34F3NO4Si3 000000-00-0 43 2 N- (Trifluoracetyl) -0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 4 Benzoic acid, ,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 Abundance Scan 1933 (22.787 min): 30935.D (-) m/ Z 73.0,0 100.00% 73
5000 147 221 355 vj-r-r-r-r-j-r-r r ' I ’ ‘ ‘ • 1 * 1 -41 281 | 2240 22.60 22.80 23.00 23.20 45 , 117. , , —— '191, eumeennut 2491 327 I 401 — m/z 147.00 26.62% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(T rifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no 73 355 5000 22.40 22.60 22.80 23.00 23.20 45 m/z 355.05 23.26% 1 1 —tTu—en—T—rr ■ i • • ■ ■ i ■ ■ ■ ■ i ■ ' ■ 1 i • 481 TTDuui 120147 193 265 ■ • ■ i ■ ' 1 1 i 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #53807; N-(Triflugracety)-0,0‘.0"tris(trimethylsilyl)epin i 73 ...... ............. ........ 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.0 16.89%
45 140 184 281 480 ‘ ‘ ‘ t • > • ■ | • miz-> 50 100 150 200 250 300 350 400 450 500 550 ......... / ______ _ Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene] ■ । ‘ । • ■ ■ • । • ■ ■ ■ । ‘ । ‘ 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.02 12.70% 5000
45 I 208 251 281 386 458 548 ■ ‘ I ’ ‘ ‘ * 1 1 1 ‘ ‘ I 1 ‘ ‘ r I *'1 ■ 1 I 1 1 1 1 I ' i ■ ■ • 1 i ■ ■ • ■ I ' 1 1 1 1 1 1 1 1 1 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30935.D GCMS1126.M Fri Jan 25 11:50:47 2002 Page 8
NYC-WTC_000018768
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NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder