Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
NYC-WTC_000018733–000018753Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51 Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 N-(Trifluoracetyl)-0,0',0"-tri Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.79 1.81 ug/1 579315 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N- (Trifluoracetyl) 0,0’ ,0"-tris (tri 495 C20H36F3NO4Si3 000000-00-0 43 2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 3 Benzoic acid, 2,6-bis[ (trimethylsil 370 C16H3004Si3 003782-85-2 38 4 Trisiloxane, ,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 Abundance Scan 1933 (22.793 min): 30934.D (-) m/ z 73.0.0 100.00% 73
5000 147 355 221 281 401 22'40 22.60 22.80 23.00 23.20 miz-> 45 — 50 117. 100 150 200 914 249. I 327 ' ■ rh Pip ■’ i* "rhi* 250 300 350 400 450 500 550 m/z 147.00 27.40% Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsilyl)epin 73 ) 355
5000 22.40 22.60 22.80 23.00 23.20 45 m/z 355.05 26.15% . I ... 140 184 281 480 ■ ■ i ■ ■ ■ • 1 ■ ■ 1 • i • ■ ■ • i ■ 1 miz-> 50 100 ' ' 150 200 250 300 350 400 450 500 550 Abundance “74702 Jerzeneethanamine, N-f(pentaflucrophenyl)methylene] 73 355 T-r-rn-r-r-j-r-r 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.0,5 18.52%
45 ____ L 208 251 281 i 386 458 548 • • i • • • • i » • • • । • • • • । • • • • / • • • • i • • • • i • • » • i • • » > i « ‘ • i » • • » i • • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy}-, trimet l ■ • • • i ■ ■ 11141s a 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.0,0 14.57% 5000
147 267 ! 47 — .208 237 1....... 1 ■ • । ■ ■ ■ ■ । ■ t ■ ■ • ■ i ■ ■ miz-> 50 100 150 200 ' ' 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30934.D GCMS1126.M Fri Jan 25 11:47:04 2002 Page 8
NYC-WTC_000018747
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NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder