Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
NYC-WTC_000018155–000018173Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30713.D Vial: 28 Acq On 1 Jan 2002 3:07 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 N-(Trifluoracetyl)-0,0',0"-tri Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T. 22.79 1.18 ug/1 464199 Phenanthrene-dl0 24.99
Hit# Of 5 Tentative ID MW MolForm CAS# Qual I N- (Trifluoracety1) -0,0' ,0"-tris (tri 495 C20H36F3NO4Si3 000000-00-0 37 2 N- (Trifluoroacetyl) -0,0' ,0' ’-tris (t 481 C19H34F3NO4Si3 000000-00-0 37 3 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 N-(Triflug^roacetyl)-N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 35 Abundance Scan 1933 (22.793 min): 30713.D (-) m/z 73.00 100.00% 73
5000 147 355 221 281 • 45 :7 117 191 | 251 — 327 , 401 41 22.40 22.60 22.80 23.00 23.20 i - 1 Pi rfin Plyi ■A -r-r -rP* ■ । ■ • ■ ■ । ■ • ■ • । ■ m/z 147.0.0 26.42% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O',O”-tris(trimethytellyl)epin 73 355 5000 1011 -PPr 22.40 22.60 22.80 23.00 23.20 45 m/z 355.0 25.63% I I h 140 184 281 480 —H ■ V. t .... । i". 1 , । • ■ ■ • । ■ ■ ■ • । ■ • ■ ■ । ■1 ■ ।' • • ■ । • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluproacety)-O.0’,O"-tris(trimethylsilyl)no 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.0,5 17.43%
45 120147 193 265 481 ■ ■ । 1 ■ ■ ■ । • • ■ • । ■ ■ ■ ■ । • • • • । ■ ■ ■ ■ । • ■ ' ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । • i ■ • * ■ । ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.0,0 14.86% 5000
45 208 251,281 251.281 . I, , , 1*1//m/00//0//nn*/0/8n/n/ 336 458 548 ■ ‘ I 1 1 —nnnn/—/K—//n/n/n/n/—/nmB—Bn/I/nn ■p-T-r-r-p-r TT-p-r-r-r-|-r-r m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30713.D GCMS1126.M Wed Jan 23 08:46:47 2002 Page 7
NYC-WTC_000018168
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NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder