GCMS analysis log for sample AD30713, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30713.D Vial: 28 Acq On 1 Jan 2002 3:07 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.89 0.51 ug/1 201540 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy- 1,1,1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 50 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 32 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 Abundance Scan 2379 (26.887 min): 30713.D (-) m/z 73.0,0 100.00% 73

5000 147 - 221 281 45 117 1911 [ 249 [ 327,355 399 429 26.60 26.80 27.00 27.20 TI’r Wt — 1*IP-T1II-+mmIT m/z 147.00 31.78% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 26.60 26.80 27.00 27.20 221 281 327 m/z 281.00 16.72% 415 519 561 ‘1** **I । > i i । i i i i । i r t i । i i ‘I Pus ■ ■ i • ■ 1 • i ■ ■ ■ • i 1 '' ' 1 i ' 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 26.60 26.80 27.00 27.20 5000 147 m/z 221.05 15.77% 34 103 281 ..... . 395 482 ■ 1 i • ■ 1 ■ i ■ 1 ■ * i • • ■ ■ i ■ ■ i ‘ • ■ i • ■ ■ ■ i 1 ' ‘ ■ i ' 1 ' ■ i 1 1 I 1 1 ' 1 I ' 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777:2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- _‘ ‘______ /________ i • ■ ■ ■ i ■ ■ • ■ I 1 1 ■ • i ■ • 73 26.60 26.80 27.00 27.20 m/z 74.00 8.60% 5000 147 45

m/z-> — 12 ■ • ‘ i1 •

50 —4 244 273 1 ! ‘ *' ! ‘ ‘ ‘ ' I ’ ‘ ‘ * I ’ ‘ 100 150 200 250 300 350 400 450 500 550 ’ I • ‘ I ‘ ’ 1 ‘ 1 1 ‘ 1 1 1 1 1 26.60 26.80 27.00 27.20

30713.D GCMS1126.M Wed Jan 23 08:46:52 2002 Page 8

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