NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30605.D Vial: 30
Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
************* ********************************************************
Peak Number 9 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
26.90 0.40 ug/1 135807 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy- 1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 59
2 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42
3 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36
4 l,l,l,5,.7<7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35
Abundance Scan 2380 (26,896 min): 30605.D (-) m/z 73.00 100.00%
73
5000
147 —................. .....................
221 281
45 191 1 249, 1 —n. —327355
117 , 401*29 26.60 26.80 27.00 27.20
TBn—r PP 1*20//n///
........ mBmOOGTITT m/z 147.00 35.31%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
5000
147 26.60 26.80 27.00 27.20
! 221 281 20- m/z 281.00 18.95%
... ...... .... ..... ............ ......... . 561
TIdr
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance 452469: Trisiloxane 1.1,1,5.5.5-hexamethyl-3.3-bisl(trimet
73 147
281 26.60 26.80 27.00 27.20
5000 m/z 221.05 15.91%
369
......... 207249
‘50 100 150 ‘200 250’ 300
338..............................
miz-> 350 400 450 500’550’ ..........................................
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
73 26.60 26*80 27.00 27.20
m/z 207.00 8.05%
207
5000 147
34 103
m/z->
' ' i ■ 1 ■ ■ i ■ ■ ..... 1I..10 ,395, 2 a MAAAAA AV, yw WWW
250 ' 300 ' ‘ 350 ‘ ‘ 400 ' 450 ' ‘ 500 “ 550 '
150 ' ‘ 200
50 100 26.60 26.80 27.00 27.20
30605.D GCMS1126.M Wed Jan 23 08:29:10 2002 Page 9
NYC-WTC_000018209
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