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GC/MS analysis results for sample AD30909, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.

NYC-WTC_000018693–000018715

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.90 1.70 ug/1 551793 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 50 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35 3 Trisiloxane, ,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 34 4 1 -Monol inolej Iglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25 Abundance 7 Scan 2380 (26.896 min): 30909.D (-) m/z 73.00 100.00% 73

5000 147 221 281 --PPPPPT 26.60 26.80 27.00 27.20 TTP 1911 1249, .. 327,355,401.429 ....... •...... 45 117 T m/z 147.00 31.79% miz-> 50 100 150 ' 200 ‘ 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 26.60 26.80 27.00 27.20 221 281 m/z 281.00 19.21% 27 415, 0519 581 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1 1.1.5.7.7.7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 1 1 i 26.60' 26.80 27.00 27.20 147 5000 267 m/z 221.05 16.47% 355 429 45 207

. ■ ■ । miz-> 50 166 150 ' 200 ' 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet ...................... 73 147 26.60 26.80 27.00 27.20 281 m/z 74.00 8.29% ! ' 5000

369 207 249,'• 338 I PIPTT ■i' " ' r ■' ■ 1 1 ■ i ■ ■ 7 ■ i ■ ■ ■ i ■ ■ ■ • t ■ ■ • ■ i ' 1 1 1 i ' 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26'80 27.00 27.20

30909.D GCMS1126.M Fri Jan 25 11:40:36 2002 Page 9

NYC-WTC_000018708

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NYC-WTC_000018708Source: NYC Law Department, mirrored locally

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