GCMS analysis results for sample AD31018, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

"Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

26.74 1.32 ug/1 422534 Phenanthrene-dl0 24.81

Hit# of 5 Tentative/ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1.1, 7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 36 2 1 -Monolinoleoyiglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36 3 1,1,1,5,7,7//-Heptamethyl-3 ,3-bis(t 444 C13H40O5Si6 038147-00-1 35 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4S15 003555-47-3 25 Abundance Scan 2363 (26.738 mln): 31018.D (-) m/ z 73.00 100.00% 73'

5000 147 221 281 .... P H, . L 249 .. 26.40 26.60 26.80 27.00 m/z-> 45 117 ■ ■!1 ■ ■ ■ । ■ ‘(■ i ■ ■ • 1 r1 191, 327355 401 429 ..... 350 400 450 500 550 m/z 147.00 33.24% 50 100 150 200 250 300 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 ................. ..... 5000 26.40 26.60 26.80 27.00 ' 147 221 281 327 m/z 281.0,0 17.30% 415 519 561 I I L m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance • • 73

207 m 26.40 26.60 26.80 27.00 5000 147 m/z " 17.26% 34 103 281 395 482 m/z-> Abundance ' 50 ' -166 ‘ -150 ' ‘ 200 ' ‘ 250 ' 300 ' 350 ' ‘ 400 ' ' 450 ' 500 ' 550 ' #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t ‘ ‘ I ‘ 4 ‘ * I ‘ ' 1 ‘ i 1 T-r-r-p-r-r-ry 73 26.40 26.60 26.80 27.00 m/z 74.00 7.43% 147 5000 267 355 429 45 207 - ■ ' i ' 1 ■ ■ i ■ ■ ■ • i ' ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 26.40 26.60 26.80 27.00

31018.D GCMS0103.M Wed Jan 09 12:08:08 2002 Page 9

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