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GCMS analysis results for sample AD31018, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017380–000017404

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017396
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NYC 9/11 Public Portal Document

Library Search Compound Report 'Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Benzoic acid, 2,4-bis[(trimeth Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

28.50 0.99 ug/1 315273 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, :2,4 bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 32 2 1-Monolinoleoy□glycerol trimethylsi 498 C27H54O4Si2 054284-45-6 30 3 N- (Trifluoroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 25 4 Benzeneethi amine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 Abundance Scan 2555 (28.500 mln): 31018.D (-) m/z 73.00 100.00% 73

5000 147 221 281 355 28.20 28'40 28.60 28.80 45 249 . L . 327. [ PI— 117 , 1914— 401 429■ i • ■ ( 0) m/z 147.00 36.47% m/z~> 50 100 150 200 250 300 ' ' 350 400 450 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsily!)oxy]-, trimet 73

5000 355 45 28.20 28.40 28.80 m/z 221.05 21.65% IT ■ 133, 193 223 ■ ■ ...... ........ miz->__ 50 100 150 ' ' '260' 250' ' ' 300 350 400 450 Abundance 73 ............. ............................ 207 28.20 28.40 28.60 28.80 5000 147 m/z 355.05 20.32% 34 103 281 395 482 m/z-> 50 100 ' ‘ 150 ‘ ‘ '260 ‘ ‘ '250‘ ' ‘ 360' ‘ ' ‘350‘ ' 400 450 ................. .................................... Abundance #58326: N-(Trifluoroacety)-o,0‘,0"-tris(trimethylsily!)no 28'20 28*40 28*60 28.80 73 355 m/z 281.00 15.32% 5000

45 — 1 126147 193 265 ......... 1376 481 , .......... /................. miz-> 50 100 150 200 250 300 350 400 450 28.20 28.40 28.60 28.80

31018.D GCMS0103.M Wed Jan 09 12:08:13 2002 Page 10

NYC-WTC_000017396

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NYC-WTC_000017396Source: NYC Law Department, mirrored locally

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