Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018445–000018469Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Benzoic acid, 2,4-bis[(trimeth Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 28.66 1.98 ug/1 1456780 Phenanthrene-dl0 24.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 2,4-bis [ (trimethylsil 370 C16H30O4Si3 010586-16-0 25 2 Benzoic acid, 2,5-bis(crimethylsilo 370 C16H30O4Si3 003618-20-0 25 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 4 Trisiloxane, 1,1,1,575,5-hexamethyl 384 C12H3604Si5 003555-47-3 17 Abundance Scan 2572 (28.655 mln): 30643.D (-) 5 m/z 73.00 100.00% 73
5000 147 221 X__________ 281 355 • ■ ■ i ■ ■ ■ ■ i ■ ■
m/z~> 45 TTr 50 117 100 PT 150 491 111/*/n//n//mnm—mTTT*0tt‘1‘’ m/z 147.00 200 249 . 1 . 327. [ 250 300 350 400 450 500 401 429 550 28.40 28.60 28.80 29.00 36.85% Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73
5000 355 T I1 T ‘I** J 28.40 28.60 28.80 29.00 45 m/z 221.05 20.83% 133 193 223 281_______ m/z-> ‘50 100 150 200 280 300 ‘ 350 ‘ 400 450 ‘ 500 ‘ 550 Abundance #73978: Benzoic acid, 2.5-bis(trimethylsiloxy)-, trimethyls 73 355 1 28.40 28.60 28.80 29.00 5000 m/z 355.05 20.80% 45 147 179 223 267 297 | FIumammmmTTmumufTmumgmmTeDTBB—ITTT miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ................ i > [ i i i i | i ill | i > > i | > i
73 28.40 28.60 28.80 29.00 m/z 281.00 16.61% 5000 147
221 21327 415 L . 519 561 1i } I I I I > I I I I TIT TT-r-r T * ‘ * I T m/z—> 50 100 150 200 250 300 350 400 450 500 550 i 28.40 28.60 28.80 29.00
30643.D GCMS1126.M Fri Feb 01 10:48:27 2002 Page 11
NYC-WTC_000018461
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NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder