GC/MS calibration data for sample 30645, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30645.D vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Benzoic acid, 2,5-bis(trimethy Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.79 3.59 ug/1 2080480 Phenanthrene-dl0 24.98

Hit# of 5 Ten .tive ID MW MolForm CAS# Qual 1 Benzoic acid 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 38 2 Benzeneeth amine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 3 N-(Trifl roacetyl)-N,0,0’,0’’-tetr 553 C22H42F3NO4S14 000000-00-0 35 4 Trisil ane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 32 Abundance Scan 1933 (22.791 mln): 30645.D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 I 22.40 22.60 22.80 23.00 23.20 45 117 191, 249,1 327 421 443 m/z-> 0 0* 1 m ei ■ ItP.ir 1* Pi’ r htri: --M*i ■ i । ■ i i i । i i i i । i 200 250 300 350 400 450 500 550 m/z 355.05 28.01% 50 100 150 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 355

5000 22.40 22.60 22.80 23.00 23.20 45 m/z 147.00 27.27% I 147 179 223 267 297 350 ' 400 ‘ 450 500 ‘ 550 miz-> 50 100 150 200 250 300 Abundance #74706: Benzeneethanamine, N-A(pentafluorophenyl)methylene] 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.95%

45 208 251 281 - 386 458 548 • • • i ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi IT T TI T T 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 15.41% 355 5000

45 147 193 — 267 ______ ________________ 538 ■ • । ■ ’i ■ ■ • • i ■ ■ ■ ■ । ' ■ i ■ ' ■ ' i" • 1 • i ■ ■ ■ • i ■ ■ ' ‘ i • ■ ’ 1 i ■ ' m/z—> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30645.D GCMS1126.M Fri Feb 01 10:53:05 2002 Page 9

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