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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018536
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Benzoic acid, 2,5-bis(trimethy Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

28.65 3.53 ug/1 2499470 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, ,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 25 2 N-(Trifluoroa etyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 25 3 3-Isopropo -1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 4 Benzeneeth.anamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 17 Abundance Scan 2571 (28.650 min): 28323.D (-) m/z 100.00% 73

5000 147 221 281 355 • ' i ‘ ‘ ' 1 I ■ ' 28.40 28.60 28.80 29.00

miz-> ' 45 —IT 50 100 117 49 249 1 327 1 401 429 t | rrs’m j i “i f । n i i i i * j i j i t j » ] t i i i j : t 150 200 250 300 350 400 450 500 550 m/z 147.00 35.20% Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 355

5000 .................. BB / \ 1Bdmdkd/d1k0/0//ok.ntn 28.40 28.60 28.80 29.00 45 m/z 221.05 20.46% | 147 179 223 267 297 • ■ i ■ ' ■ • i • ■ ■ 1 ■ ■ 1 ■ i ■ ■ ■ ■ i ■ ■ J ' i ■ ' ' i ■ 1 ■ ■ i ■ ■ ■ ■ i ■ ■ • • i ■ ■ ■ ■ i • ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #rr 162 -{Trflvorcacety)-N.’ ' '■ thni smimainyis 73 - 355 28.40 28.60 28.80 29.00 5000 19.31%

45 147 193 267 538 m/z-> 50 100 150 200 250 300 350 400 450 500 550 ’ Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 28.40 28.60 28.80 29.00 m/z 281.00 15.43% 5000 147

... 327.415. ,595* miz-> 50 ' 100 ‘ '156 ‘ ' 200 ' ‘ 250 ' ' 300 350 ' 400 ' ‘ 450 ' 500 550 ' 28.40 28.60 28.80 29'00

28323.D GCMS1126.M Wed Feb 06 13:02:16 2002 Page 12

NYC-WTC_000018536

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NYC-WTC_000018536Source: NYC Law Department, mirrored locally

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