Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018519–000018545Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 30.25 6.71 ug/1 2358560 Chrysene-dl2 33.02 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 36 2 Trisiloxane, 1,1,1,5, 5,5-hexamethyl 384 C12H3604S15 003555-47-3 32 3 3-1 sopropoxy -1,1,1, 7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 4 Benzoic acid. 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 22 Abundance (.... Scan 2745 (30.248 mln): 28323.D (-) m/z 73.00 1 00.00% 73
5000 147 221 ■ ■ i ' ' 281 355 ■ • i ■ ■ 30.00 30.20 30.40 30.60 45 04 ■ 1 4 r 117. +1914 249, .. 401 429 11—PmmeIT I m/z 147.00 37.61% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 -r-j-r-n-r-p-r 5000 267 ■ ■ i ' • 355 426 30.00 30.20 30.40 30.60 45 207 m/z 221.05 22.37% ‘ ' I ‘ ‘ ‘ ■ I ■ • ‘ • I ‘ ‘ ‘ ‘ I ' • ‘ ' I ‘ ‘ f I ' ‘ ‘ • I ■ ‘ ‘ ‘ I ' ‘ ‘ ‘ I ‘ ‘ I ‘ ‘ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1 ,5,5,5-hexametn,"3 3-bisittrimet 73 147 ■ ■ i ■ ■ ... ‘ ■ i ■ • 281 30.00 30.20 30.40 30.60 5000 m/z 355.05 15.23% 369 207 249 । 338 | m/z~> 50 100 150 ‘ 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim • • i • • ’ t* 73 30.00 30.20 30.40 30.60 rn/z 281.00 13.79% 5000 147 221 281 327 415 519 561 ■ • i ■ ‘ ■ i ■ • • ■ i ■ 1 ■ ■ i • r ■ ■ i ■ * ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 • ■ ■ i Tr • i ' • ‘ ' l ‘ ‘ 1 ■ i ‘ ‘ m/z~> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60
28323.D GCMS1126.M Wed Feb 06 13:02:21 2002 Page 13
NYC-WTC_000018537
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
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