GC/MS calibration data for sample 30643, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 30.24 3.03 ug/1 1359020 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW Mol Form CAS# Qual 1 1,1,1,5,7,7,7-Heptamethy]-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 2 Benzoic acid, 2,4-bis [ (trimethylsil 370 C16H30O4Si3 010586-16-0 30 3 3-Isopropoxy-1,1,1,7,7/7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Tris(trimethylsilyl)bprate 278 C9H27BO3Si3 004325-85-3 14 Abundance Scan 2745 (30.243 min): 30643.D (-) m/ z 73.0,0 100.00% 73

5000 147 221 । । । n . । f> Stt । i i । । । । । 281 355 429 30.00 30.20 30.40 30.60 .. 191 45 117 TI *I* TPefr Pi 249-1+3274401 -........................ ... ■ m/z 147.00 35.56% mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bls(trimethylsiloxy)t 73 147 ------- 5000 267 355 429 30.00 30.20 30.40 30.60 45 207 m/z 221.0 20.37% • • ■ i ...... It I 1 ■ i ■ ■ ■ • i • ■ • ' i ■ ■ ■ • i • ■ ■ ■ i • • i ■ • ■ ■ i ■ • ■ i ■ ‘ ■ ■ i ■ ■ • ■ i • ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid. 2.4-bis[(trimethylsilyl)oxy]- trimet 73 TT~p-r ‘ ‘ l • ’ 30,00 30.20 30.40 30.60 5000 355 m/z 355.05 13.28% 45 133 193 223 281 TEIBBBBB/-—TTTTTTTTTTTTTTIGIT miz-> 50 100 150 200 250 300 350 400 450 500 550 ---------- Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 30.00 30.20 30.40 30.60 m/z 281.00 12.17% 5000 147 221 281 •’I’I4*I’I*8* ’ i I 144 1‛II Idrnn—nmnnm——Bn—Bn-m 327, 415 519 561 1 » j I i i f i I’r i j i i i i । । > m/z—> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60

30643.D GCMS1126.M Fri Feb 01 10:48:31 2002 Page 12

NYC-WTC_000018462