Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
30.25 1.49 ug/1 610596 Chrysene-dl2 33.03
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 27 3 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 4 Tris(trimethylsilyl)borate ______ 278 C9H27B03Si3 004325-85-3 12 Abundance Scan 2745 (30.246 min): 30650.D (-) m/ z 73.0,0 100.00% 73
5000 147 221 ' ' i n ' ■ I ' ' 1 ■ i ■ ' ‘ ■ i ' ' | 281 30.00 30.20 30.40 30.60 45 117. , 1911 .249 1 , 327 355 401 429 ' '‘I 1 r ivan" ■ i ‘ । i r pi r । i [ in r i‘| 7 । । ' । । P| । ' PP1 1 I r-r m/z 147.00 37.03% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 T-n-rr 147 30.00 30.20 30.40 30.60 m/z 221.05 20.76% 271 21 327 TTIPTITITImIUIIII415 519 561 m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid 2.4 bisfgmnethy’silyl)oxy]-. trimet 73 ■ ■ । 1 1 30.00 30.20 30.40 30.60 5000 355 m/z 355.05 12.75% 45 133 193 223 281 i ■ ■ ■ j ■ m/z-> 50 100 150 200_ 250 300__ 350 _ 400 450 500__ _550 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 30.00 30.20 30.40 30.60 m/z 281.00 12.44% 147 5000 267 355 429 45 207
■ ‘ I i l I m/z-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60
30650.D GCMS1126.M Mon Jan 28 11:18:48 2002 Page 11
NYC-WTC_000004381
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
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