Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
28.66 1.08 ug/1 678263 Phenanthrene-dl0 24.99
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 16 3 3-1sopropoxy 71, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 16 4 Benzoic acid , 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 12 Abundance Scan 2572 (28.658 min): 30650.D (-) m/ z 73.0,0 100.00% 73
40 5000 147 221 355 281 327 401 429 28.40 28.60 28.80 29.00 117 I ’ 1 1 ■' 1 1 7.4 . , 1911 +,249- •' ■ । 1 ■ ■ ■ । ' ‘ । ■ m/z 39.90 53.32% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 28.40 28.60 28.80 29.00 369 m/z 147.00 31.27% 207 I 249 1. I. 338 I m/z-> 50 100 150 __ 200 250 300 350 400 450 500 550 Abundance #74706: Benz neethenamine, N-f(pentafluorophenylimethylene] 73 355 28.40 28.60 28.80 29.00 5000 m/z 355.05 28.39%
45 208 251 281 | 386 458 548 m/z-> Abundance 50 100 150 200 250 300 350 400 450 #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 500 550
73 28.40 28.60 28.80 29.00 m/z 221.05 28.10% 5000 147
m/z—> . .. . 221 21 327 50 100 150 200 250 300 350 415
400 1 450 500 519 550 561 28.40 28.60 28.80 29.00
30650.D GCMS1126.M Mon Jan 28 11:18:43 2002 Page 10
NYC-WTC_000004380
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
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