NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results for sample AE02575, March 2002
Machine-extracted title · confidence 90%Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
NYC-WTC_000038871–000038890Folder label: “GCMS X 3/4/02 A 3/20/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR1902\2575.D Vial: 24 Acq On : 21 Mar 2002 3:41 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
29.26 0.26 ug/1 55464 Phenanthrene-dl0 25.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, A,1,5,5,5-hexamethyl 384 C12H36O4S15 003555-47-3 43 2 3-Isopropoxy- 11, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 16 4 Phenethylaminl , N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 12 Abundance / Scan 2637 (29.257 min): 2575.D (-) m/ Z 73.00 100.00%
5000 I CP 147 221 281 355 ---................. ■ 45 , 325 j 401 429 29.00 29.20 29.40 29.60 117, — T 11 ' TTN—mT m/z 147. 0.0 43.72% m/z- _ 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyi-3,3-bisi(trimet 73 147 281 5000 -...... 29.00 29.20 29.40 29.60 369 m/z 355.05 30.99% ------------ ' I 207 249 I L , —338—.......... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance . wpppuki 73 —.... 4.... H 29.00 29.20 29.40 29.60 5000 147 m/z 221.05 27.14%
221 281 327 415 519 561 1 1 । ‘ ■ * 1 । ■ 1 mz-2.__ 50 100 150 200 250 300 350 400 1450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl )oxy]-, trimet —..4.... 73 29.00 29.20 29.40 29.60 m/z 281.00 25.02% 5000 355 45 133 193 223 281 I l li, m/z-> 50 100 150 200 250 300 350 400 450 500 550 29.00 29.20 29.40 29.60
2575.D GCMS0308.M Thu Mar 21 14:23:59 2002 Page 9
NYC-WTC_000038886
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