NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS blank analysis results, Mar 13, 2002
Machine-extracted title · confidence 90%Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
NYC-WTC_000005367–000005382Folder label: “GCMS X 2/5/02 A 3/7/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR0702\LB.D Vial: 15 Acq On : 8 Mar 2002 3:29 am Operator: Sample : gc/ms scan 2/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
27.52 0.20 ug/1 33925 Phenanthrene-dl0 25.69
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,11, 5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 50 2 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 33 4 Ethanedioic /acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 17 Abundance 73 Scan 2448 (27.521 min): LB.D (-) m/z 73.00 100.00%
5000- 147 221 281
■ 45 ‘‘i ■ ■ J 355 Im 429 27.20 27.40 27.60 27.80 m/z 147.00 39.67% m/z-2 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiioxane. 1,1,1,5,5,5-hexamethyi-3,3-bis[(trimet 73 147
281 5000- 27.20 27.40 27.60 27.80 369 m/z 281.10 22.58% 1 207 ppjanct .. 1, 249 338 1........... m/z->50 100 150 200 250 300 350 400 450 500 550 Abundance 73
207 27.20 27.40 27.60 27.80 5000 147 m/z 221.05 21.51% 34 103 281
50 100 150 200 250 300 350 395, 400 ..... 450 482500.550 ______ Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 27.20 27.40 27.60 27.80 m/z 355.05 9.36% 5000 147
221 281 327 415 ..... .................. !...... ) 1 ....... 417......... 519 561 i ■ ■ ’ ■ i ‘ ■ ■ ■ i m/z-> 50 100 150 200 250 300 350 400 450 500 550 27.20 27.40 27.60 27.80
LB.D GCMS0208.M Wed Mar'13 15:04:05 2002 Page 8
NYC-WTC_000005380
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NYC-WTC_000005380Source: NYC Law Department, mirrored locally
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