GCMS blank analysis results, Mar 13, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0 7 02\LB.D Vial: 15 Acq On 8 Mar 2002 3:29 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Ethanedione, diphenyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

33.46 0.22 ug/1 34987 Chrysene-dl2 33.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanedione, diphenyl- 210 C14H10O2 000134-81-6 10 2 Benzenepentanoic acid, .delta.-oxo- 192 C11H1203 001501-05-9 10 3 1,2-Bis(benzoyloxy)benzene 318 C20H14O4 000643-94-7 10 formyloxybenzene 4 1-Benzoyloxy-2-/ Scan 3095 (33.461 min): LB.D (-) 242 C14H10O4 797922-93-1 10 Abundance .. m/z 104.90 100.00% 405 149

5000- 77 / S , । -I , , 51 33.20 33.40 33.60 33.80 207 ' i ■ m/z 149.00 77.35% m/z-?_ 2Q.... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #70180: Ethanedione, diphenyl- 105

5000 77 L 33.20 33.40 33.60 33.80 51 m/ z j | 178 210 I’’’’!’ ■ ■ ■ i ' ' ■ 'i ■ ■ ' ' i ' ' '' i '' ' ' i''' ' i '1 ■ ‘ i '' ‘' i' ' '' i T’I i' ' ‘ ■ i ' '' ■ i TT‘ m/Z->20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance . - o llto ■ 105 .......... A ’ I’’’ 33.20 33.40 33.60 33.80 5000- 77 m/z 51.00 10.14%

51 192 27 120 146 i1 ' i ■ ■ ■' i ■' ■ ■ i ‘ ' i ■ '' ■ i '''11 ■ ■' ■ i ' '' ' i ■ ■1' i ■ ■ ■ ■ i' ■ ■ ■ i'1 ■ ■ i'1 ■ ■ i ■ ■' ■ i ■ ■ ■ ■ i ■ ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #45379: 1,2-Bis(benzoyloxyjbenzene 105 33.20 33.40 33.60 33.80 m/ z 150.00 8.51% 5000 77

51 27 121 137 197 213 318 । > 111 ■ l > । > TIT 11 —209100111011110001101. i' ■ ■ ■ i' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ 'i ■' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 33.20 33.40 33.60 33.80

LB.D GCMS0208.M Wed Mar' 13 15:04:09 2002 Page 9

NYC-WTC_000005381