GCMS analysis results for sample AE02581, Mar 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0702\2581.D Vial: 24 Acq On 8 Mar 2002 12:21 pm Operator: Sample re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Ethanedione, diphenyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.45 0.27 ug/1 50877 Chrysene-dl2 33.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanedione, diphenyl- 210 C14H10O2 000134-81-6 25 2 1,2 -Bis (benzoyloxy) benzene 318 C20H14O4 000643-94-7 25 3 Benzai ide, N-propyl- 163 C10H13NO 010546-70-0 25 _ 4 1-Pro anone, 2,2-dichloro-3-hydroxy 218 C9H8C12O2 054824-08-7 25 Abundance Scan 3095 (33.454 min): 258LD (-) m/z 104.95 100.0 0 % 105 149

5000 77

51 163 33.20 33.40 33.60 33.80 I 207 1111 u 1 11 " p * * ■ ।' •r-’ r* ° ■ i • •1 ■ p "‘‘16847} i > 111।। ■ i' ■ ■ ■ i ■ ■' ■ i ■ ■ m/z 149.00 72.59% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #70181: Ethanedione, diphenyl- 105

- 5000 77 33.20 33.40 33.60 33.80 51 m/z 77.05 37.10% 27 .1 151 210 11′3 11 1 11 1 1' m/z-2 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 105

33.20 33.40 33.60 33.80 5000 77 m/z 51.00 10.68%

27 51 121 137 197 213 318 T‘11‘1‘011111111111101t00——BnEuuuum3‘T71mUIIT‘T m/z-2_ 20_40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 - Abundance #13165: Benzamide, N-propyl- 105 33.20 33.40 33.60 33.80 m/z 150.00 7.63% 5000 A 77 163

m/z--> 51 J i ■1 ■ ■ i ■ ■ ■ ■ i ■ 20 40 60 1 ... .... 134148, ........ 80 100 120 140 160 180 200 220 240 260 280 300 320 .... Ill... L. 33.20 33.40 33.60 33.80

2581.D GCMS0208.M Wed Mar 13 14:47:38 2002 Page 3

NYC-WTC_000005392