GCMS analysis results for sample AE02581, Mar 15, 2002

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Data File C:\HPCHEM\1\DATA\MAR0 702\2581.D Vial: 24 Acq On 8 Mar 2002 12:21 pm Operator: Sample re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.82 0.20 ug/1 40487 Phenanthrene-dl0 25.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- X 188 C14D10 001719-06-8 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 91 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 4 4-Fluoro-6-methyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 36 Abundance Scan 2264 (25,825 min): 2581.D (-) m/ z 18 .10 100.00% 188

5000

Tik,T ‘ ■ i ■ ■ ■ ■ i ■ ■ 25.40 25.60 25.80 26.00 26.20

m/z-? 4252668094 ...... 146 158... 1. — TTTTTT*TDmWIITTRPWTRTTIPTT 4050 60 70 80 90 100. 110 120 130 140 150 160 170 180 190 m/ Z 18 .05 13.90% Abundance #19957: Anthracene-d10- 188

5000 25.40 25.60 25.80 26.00 26.20 m/ z 18 .10 12.24%

m/Z-?__ 66 111" " 111111" ।1111" 1" 80 94 i''‘ i ■ ■'' i' ‘ • i ■' ■ ■ i TT-p-n-rp- 40 50 60 70 80 90 100 110 120 130 .140 150 160 170 180 190 160 +— Abundance 188

25.40 25.60 25.80 26.00 26.20 5000 m/z 9 . 00 11.86% 80 94 160 66 a m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .......................... ........................... Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 25.40 25.60 25.80 26.00 26.20 m/z 80.00 10.84% 5000 102 115 145

'■। 51 -1 ■ ■ ■ ■ j 63 75 94 . i' ri 111111111'' । TTIHTu 130 '' i' ‘ 158 H ' i ■ ■ ■11 ■ ■ ■' i ■ I IUr 1 25.40 25.60 25.80 26.00 26.20 m/z--> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190

2581.D GCMS0208.M Wed Mar 13 14:47:33 2002 Page 2

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